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ThermoFisher賽默飛離子色譜儀的基本操作步驟
發布時間： 2020-11-26 點擊次數： 8141次離子色譜儀以ThermoFisher賽默飛*離子色譜技術為依托，專門為滿足用戶常規陰、陽離子檢測需要而設計。配備有雙柱塞泵，可兼容電解或化學連續再生微膜抑制器。采用變色龍軟件操控，具有操作簡單、啟動快速、性能可靠穩定等特點。儀器操作者只需經過簡單培訓就可進行獨立操作，維護成本極低。系統特點：1、采用交聯特氟龍材質鋁管作為采樣管，將顆粒物損失降至zui低；2、自動化程度高、操作維護簡便，簡單設置即可實現自動在線監測，并同時檢測氣溶膠和氣體組分鐘的陰陽離子；3、進樣體積小，能夠實現較高的靈敏度，色譜柱壽命長，相對成本低；4、采用抑制技術，ji大提高了靈敏度，可檢測極低濃度的組分；5、采用陽離子抑制技術，能否開拓更多的檢測項目，如Li+、Sr2+和Ba2+等離子；6、顆粒物和氣體均采用陰陽離子分流的進樣方式，避免了交叉污染，結果準確。ThermoFisher賽默飛離子色譜儀的基本操作步驟：1、開機前的準備：打開實驗室空調，根據樣品的檢測條件和色譜柱的條件配置所需淋洗液和再生液。2、開機：依次打開打印機、計算機進入操作系統；打開氮氣鋼瓶總閥，調節鋼瓶減壓閥分壓表指針為0.2MPa左右，再調節色譜主機上的減壓表指針為5psi左右，確認離子色譜儀與及計算機數據線連接正常，打開離子色譜主機電源；點擊開始、程序、Chromeleon、severmonitor、雙擊桌面上工作站程序、雙擊安裝目錄下離子色譜操作控制面板；操作控制面板打開后選中connected使軟件與離子色譜儀聯動起來，打開泵頭廢液閥排除泵和管路里的氣泡，關閉泵頭廢液閥，開泵啟動儀器，查看基線，待基線穩定后方可進樣分析。3、樣品分析：建立程序文件；建立方法文件；建立樣品表文件；加樣品到自動進樣器或手動進樣；啟動樣品表；若是手動進樣，按系統提示逐個進樣分析。4、數據處理：建立標準曲線；打印標準曲線；打印待測樣品分析報告。5、關機：關閉泵，關閉操作軟件；關閉離子色譜主機電源；關閉氮氣鋼瓶總閥并將減壓表卸壓；關閉計算機、顯示器和打印機電源。
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